D a t a   F i l e   C : \ C H E M 3 2 \ 1 \ D A T A \ M A R I O \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 6 - 4 5 - 3 1 \ B E N Z O S _ 2 5 0 P P M . D 
 
 S a m p l e   N a m e :   b e n z o s _ 2 5 0 p p m 
 
 I n s t r u m e n t   1   6 / 2 1 / 2 0 2 3   5 : 4 6 : 5 7   P M   M a r i o 
 
 
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
 A c q .   O p e r a t o r       :   M a r i o                                                     S e q .   L i n e   :       1 
 
 A c q .   I n s t r u m e n t   :   I n s t r u m e n t   1                                         L o c a t i o n   :   V i a l   2 
 
 I n j e c t i o n   D a t e     :   6 / 2 1 / 2 0 2 3   4 : 4 6 : 4 0   P M                                   I n j   :       1 
 
                                                                                                 I n j   V o l u m e   :   1 5 . 0    l 
 
 S e q u e n c e   F i l e       :   C : \ C h e m 3 2 \ 1 \ D A T A \ M a r i o \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 6 - 4 5 - 3 1 \ B X _ S T D S _ E B _ 
 
                                     0 6 2 0 2 0 2 3 . S 
 
 M e t h o d                     :   C : \ C H E M 3 2 \ 1 \ D A T A \ M A R I O \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 6 - 4 5 - 3 1 \ E T H A N _ D T _ 
 
                                     M E O H _ L 1 6 - 6 . M   ( S e q u e n c e   M e t h o d ) 
 
 L a s t   c h a n g e d         :   6 / 5 / 2 0 2 3   1 0 : 4 9 : 1 0   A M   b y   M a r i o 
 
 M e t h o d   I n f o           :   S o l i d a g o   p h e n o l i c s   a n d   d i t e r p e n e   a c i d   a n a l y s i s 
 
 
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
                                                   A r e a   P e r c e n t   R e p o r t                                                   
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
 
 
 S o r t e d   B y                           :             S i g n a l 
 
 M u l t i p l i e r :                                       :             1 . 0 0 0 0 
 
 D i l u t i o n :                                           :             1 . 0 0 0 0 
 
 U s e   M u l t i p l i e r   &   D i l u t i o n   F a c t o r   w i t h   I S T D s 
 
 
 
 
 
 S i g n a l   1 :   D A D 1   A ,   S i g = 2 5 4 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       1 . 9 4 8   B B         0 . 2 4 8 3     1 4 0 . 9 5 9 2 4         7 . 0 7 8 9 0       0 . 5 6 9 8 
 
       2       2 . 3 7 3   B V         0 . 1 4 3 3     1 6 1 . 7 4 5 1 9       1 4 . 5 9 6 2 2       0 . 6 5 3 9 
 
       3       2 . 5 1 7   V V         0 . 0 9 1 2     1 0 8 . 1 1 9 0 0       1 6 . 7 7 6 5 1       0 . 4 3 7 1 
 
       4       2 . 6 6 9   V V         0 . 0 7 5 2     1 0 2 . 5 4 3 8 2       2 1 . 6 5 7 3 2       0 . 4 1 4 5 
 
       5       2 . 7 6 9   V B         0 . 1 6 1 2     3 8 9 . 2 5 2 1 1       3 1 . 2 6 7 1 6       1 . 5 7 3 6 
 
       6       3 . 8 9 8   B V         0 . 7 9 7 3   1 2 1 1 . 7 6 7 7 0       1 8 . 4 2 3 8 4       4 . 8 9 8 7 
 
       7       5 . 0 6 3   V V         0 . 4 2 1 1     3 8 2 . 3 5 2 5 1       1 1 . 6 4 3 9 8       1 . 5 4 5 7 
 
       8       5 . 3 1 9   V V         0 . 2 2 4 4     1 6 0 . 0 9 9 7 5       1 0 . 3 5 2 3 9       0 . 6 4 7 2 
 
       9       5 . 6 1 5   V V         0 . 2 6 3 3     1 9 2 . 4 0 6 1 0         9 . 9 6 3 9 9       0 . 7 7 7 8 
 
     1 0       6 . 1 0 8   V V         0 . 4 3 9 8     3 3 5 . 4 3 1 4 0         9 . 2 7 8 2 0       1 . 3 5 6 0 
 
     1 1       6 . 6 2 1   V B         0 . 4 3 6 0     2 8 3 . 1 8 0 4 8         7 . 9 0 4 3 9       1 . 1 4 4 8 
 
     1 2       7 . 2 2 3   B V         0 . 3 0 6 0     1 5 8 . 8 2 7 5 8         6 . 8 1 2 9 9       0 . 6 4 2 1 
 
     1 3       7 . 9 1 6   V V         0 . 7 9 4 6     3 5 6 . 5 0 8 7 3         5 . 7 5 6 3 5       1 . 4 4 1 2 
 
     1 4     1 2 . 5 4 1   V B         0 . 3 1 4 2   7 0 7 8 . 1 5 2 8 3     3 4 9 . 5 5 1 4 2     2 8 . 6 1 4 3 
 
     1 5     1 4 . 2 0 3   B V         0 . 6 1 1 9     1 3 6 . 6 2 7 7 0         2 . 8 2 6 9 7       0 . 5 5 2 3 
 
     1 6     1 7 . 7 5 4   B V         0 . 4 0 2 3       7 8 . 4 7 8 8 7         2 . 8 7 6 1 1       0 . 3 1 7 3 
 
     1 7     1 9 . 0 6 8   V B         0 . 3 7 2 1   1 . 0 9 5 4 2 e 4       4 5 6 . 2 2 1 5 6     4 4 . 2 8 3 8 
 
     1 8     2 0 . 9 7 9   B B         0 . 3 6 5 2   1 8 0 6 . 6 4 5 3 9       7 6 . 0 5 0 5 7       7 . 3 0 3 6 
 
     1 9     2 8 . 2 2 5   B B         0 . 3 5 8 7     6 3 7 . 8 3 0 3 8       2 7 . 4 9 3 3 2       2 . 5 7 8 5 
 
     2 0     3 6 . 6 4 3   B B         0 . 5 2 4 6       6 1 . 2 5 1 5 5         1 . 6 2 1 9 1       0 . 2 4 7 6 
 
 T o t a l s   :                                     2 . 4 7 3 6 4 e 4     1 0 8 8 . 1 5 4 1 0 
 
 
 
 
 
 S i g n a l   2 :   D A D 1   C ,   S i g = 3 2 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 3 7 0   B V         0 . 1 1 1 5       9 6 . 8 4 4 5 8       1 1 . 8 3 1 0 0       6 . 9 1 1 4 
 
       2       2 . 5 0 2   V V         0 . 0 9 9 2     1 0 7 . 6 3 1 4 7       1 6 . 6 8 9 0 2       7 . 6 8 1 2 
 
       3       2 . 6 6 4   V V         0 . 0 7 4 0     1 0 3 . 8 1 0 3 7       2 2 . 4 0 8 7 4       7 . 4 0 8 5 
 
       4       2 . 7 6 3   V B         0 . 1 1 6 5     2 4 8 . 6 0 3 3 9       2 9 . 4 5 2 5 6     1 7 . 7 4 1 8 
 
       5       3 . 8 8 1   B V         0 . 5 8 8 8     2 8 9 . 2 7 1 1 5         6 . 7 9 3 1 5     2 0 . 6 4 4 1 
 
       6       5 . 0 6 6   V B         0 . 3 2 7 8     1 3 2 . 7 1 8 2 9         5 . 3 8 0 9 2       9 . 4 7 1 6 
 
       7       5 . 6 0 2   B V         0 . 2 6 2 0       5 9 . 0 5 8 6 0         3 . 1 8 9 7 4       4 . 2 1 4 8 
 
       8     1 2 . 5 0 8   B B         0 . 3 3 9 7       2 5 . 5 0 6 6 4         1 . 1 0 3 1 8       1 . 8 2 0 3 
 
       9     1 4 . 2 0 1   B B         0 . 5 5 6 5     1 4 2 . 0 2 5 7 4         3 . 5 6 7 1 6     1 0 . 1 3 5 8 
 
     1 0     1 9 . 0 6 6   B B         0 . 3 6 1 7     1 9 5 . 7 5 9 6 3         8 . 1 0 7 1 7     1 3 . 9 7 0 6 
 
 T o t a l s   :                                     1 4 0 1 . 2 2 9 8 7     1 0 8 . 5 2 2 6 6 
 
 
 
 
 
 S i g n a l   3 :   D A D 1   D ,   S i g = 3 6 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       0 . 5 1 6   B V         0 . 4 5 4 1       9 6 . 4 4 8 0 4         2 . 8 9 9 5 3       2 . 4 0 2 1 
 
       2       2 . 3 6 9   B V         0 . 3 4 9 8     5 7 4 . 0 0 1 8 3       2 0 . 0 6 0 6 2     1 4 . 2 9 5 7 
 
       3       2 . 5 0 0   V V         0 . 0 9 6 8     1 3 1 . 1 4 8 8 8       2 0 . 4 4 7 4 5       3 . 2 6 6 3 
 
       4       2 . 6 6 4   V V         0 . 0 7 4 6     1 2 6 . 3 4 1 9 1       2 6 . 9 8 9 4 9       3 . 1 4 6 6 
 
       5       2 . 7 6 0   V B         0 . 1 3 9 0     3 9 2 . 2 7 8 1 4       3 7 . 2 1 1 3 6       9 . 7 6 9 8 
 
       6       3 . 8 6 8   B V         0 . 8 1 9 7   1 3 2 2 . 8 1 9 5 8       2 0 . 6 9 4 6 0     3 2 . 9 4 5 2 
 
       7       5 . 0 7 0   V V         0 . 4 3 2 2     4 0 9 . 0 6 1 7 4       1 2 . 1 6 7 2 4     1 0 . 1 8 7 8 
 
       8       5 . 6 0 0   V V         0 . 4 0 0 8     3 3 4 . 8 4 7 0 5       1 0 . 3 1 3 7 8       8 . 3 3 9 5 
 
       9       6 . 6 2 2   V V         0 . 8 4 6 4     5 1 0 . 9 7 2 2 3         7 . 1 6 1 2 9     1 2 . 7 2 5 9 
 
     1 0     1 4 . 2 1 6   B V         0 . 6 1 4 4     1 1 7 . 2 9 7 3 3         2 . 5 2 2 9 8       2 . 9 2 1 3 
 
 T o t a l s   :                                     4 0 1 5 . 2 1 6 7 3     1 6 0 . 4 6 8 3 5 
 
 
 
 
 
 S i g n a l   4 :   D A D 1   E ,   S i g = 2 1 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       1 . 9 5 0   B V         0 . 1 4 5 4       6 5 . 6 9 6 0 8         5 . 7 4 5 1 1       0 . 0 8 3 0 
 
       2       2 . 1 3 3   V V         0 . 1 5 2 1       8 4 . 8 4 8 1 2         7 . 2 7 1 9 0       0 . 1 0 7 1 
 
       3       2 . 3 7 2   V V         0 . 1 3 0 6       7 0 . 4 6 4 0 3         7 . 1 7 3 7 4       0 . 0 8 9 0 
 
       4       2 . 5 2 8   V V         0 . 0 8 8 2       5 2 . 7 2 1 2 8         8 . 5 1 3 3 7       0 . 0 6 6 6 
 
       5       2 . 6 6 8   V V         0 . 0 7 3 8       5 1 . 7 2 9 5 2       1 1 . 2 1 5 8 4       0 . 0 6 5 3 
 
       6       2 . 7 6 9   V B         0 . 1 3 0 8     1 6 5 . 6 8 9 5 3       1 6 . 8 4 5 0 1       0 . 2 0 9 2 
 
       7       3 . 8 5 5   B V         0 . 4 5 0 5     2 9 1 . 8 4 8 1 8         8 . 0 5 8 2 0       0 . 3 6 8 5 
 
       8       4 . 1 3 3   V V         0 . 1 9 7 8     1 1 4 . 1 8 0 3 4         7 . 6 6 4 0 5       0 . 1 4 4 2 
 
       9       5 . 0 6 1   V V         0 . 1 8 5 8     1 6 9 . 2 6 2 2 1       1 3 . 5 4 4 0 0       0 . 2 1 3 7 
 
     1 0       5 . 6 0 1   V V         0 . 1 9 4 2       5 4 . 1 7 9 9 5         4 . 2 0 7 6 5       0 . 0 6 8 4 
 
     1 1       6 . 0 6 1   V V         0 . 5 6 0 7     2 8 8 . 0 9 3 8 4         7 . 1 1 0 2 5       0 . 3 6 3 8 
 
     1 2       7 . 8 8 2   V V         0 . 5 2 2 6     2 4 4 . 2 8 9 6 1         5 . 9 0 5 9 0       0 . 3 0 8 5 
 
     1 3       9 . 1 1 9   V V         0 . 6 6 8 1     3 9 9 . 8 0 2 7 0         7 . 6 2 0 7 2       0 . 5 0 4 9 
 
     1 4       9 . 5 9 1   V V         0 . 3 4 1 0     1 7 8 . 1 1 5 7 8         7 . 1 8 9 9 6       0 . 2 2 4 9 
 
     1 5     1 0 . 1 5 3   V B         0 . 7 3 6 3     3 9 4 . 0 9 2 5 6         6 . 7 1 9 3 7       0 . 4 9 7 6 
 
     1 6     1 1 . 8 9 5   B V         0 . 3 4 6 7     1 7 1 . 4 4 0 4 1         6 . 9 7 5 6 7       0 . 2 1 6 5 
 
     1 7     1 2 . 5 4 1   V B         0 . 3 1 9 6   1 . 9 5 6 9 6 e 4       9 5 2 . 7 1 9 2 4     2 4 . 7 1 1 5 
 
     1 8     1 4 . 1 8 4   B V         0 . 5 2 6 2     5 9 5 . 6 4 8 3 8       1 6 . 7 7 6 0 4       0 . 7 5 2 2 
 
     1 9     1 5 . 3 3 8   V B         0 . 3 2 3 4       2 7 . 3 7 2 1 5         1 . 0 9 5 7 6       0 . 0 3 4 6 
 
     2 0     1 7 . 7 4 8   B V         0 . 3 9 7 0     1 6 0 . 5 9 3 7 5         6 . 4 8 2 1 9       0 . 2 0 2 8 
 
     2 1     1 9 . 0 6 9   V V         0 . 3 7 9 3   2 . 9 2 0 4 1 e 4     1 2 0 2 . 6 2 3 5 4     3 6 . 8 7 7 5 
 
     2 2     2 0 . 9 7 8   V B         0 . 3 6 2 1   1 . 3 5 9 5 2 e 4       5 7 8 . 5 7 5 7 4     1 7 . 1 6 7 4 
 
     2 3     2 4 . 9 0 7   B B         0 . 5 6 9 5       4 2 . 3 5 7 7 2   9 . 6 2 4 0 2 e - 1       0 . 0 5 3 5 
 
     2 4     2 8 . 2 2 5   B B         0 . 3 6 4 7   1 . 3 1 0 9 1 e 4       5 6 0 . 9 2 8 8 9     1 6 . 5 5 3 5 
 
     2 5     3 6 . 6 2 2   B V         0 . 3 7 6 6       9 1 . 7 7 9 0 9         3 . 7 1 0 7 2       0 . 1 1 5 9 
 
 T o t a l s   :                                     7 . 9 1 9 2 2 e 4     3 4 5 5 . 6 3 5 2 8 
 
 
 
 
 
 S i g n a l   5 :   D A D 1   B ,   S i g = 2 3 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       0 . 4 8 8   B V         0 . 5 5 4 2       6 8 . 8 0 8 2 0         1 . 5 6 1 1 0       0 . 1 8 1 1 
 
       2       1 . 0 5 0   V B         0 . 5 6 8 1     2 2 0 . 3 7 2 1 0         4 . 6 2 3 3 3       0 . 5 8 0 0 
 
       3       2 . 1 3 0   B V         0 . 3 0 3 4     2 7 6 . 3 7 1 6 7       1 1 . 3 7 6 4 6       0 . 7 2 7 4 
 
       4       2 . 3 7 5   V V         0 . 1 4 2 9     1 4 3 . 4 8 4 1 2       1 3 . 1 9 6 1 7       0 . 3 7 7 7 
 
       5       2 . 5 2 4   V V         0 . 1 1 1 1       9 3 . 1 2 8 4 7       1 3 . 9 6 6 2 7       0 . 2 4 5 1 
 
       6       2 . 6 7 0   V V         0 . 0 7 4 1       7 6 . 9 8 0 8 1       1 6 . 6 0 3 4 2       0 . 2 0 2 6 
 
       7       2 . 7 7 2   V B         0 . 1 9 0 5     3 7 6 . 9 2 3 3 7       2 5 . 1 9 5 5 2       0 . 9 9 2 1 
 
       8       3 . 9 0 1   B V         0 . 8 6 6 2   1 0 4 4 . 8 6 3 1 6       1 5 . 0 4 5 0 1       2 . 7 5 0 1 
 
       9       5 . 0 6 3   V V         0 . 4 0 1 9     3 4 2 . 3 5 3 7 3       1 1 . 0 3 7 9 3       0 . 9 0 1 1 
 
     1 0       5 . 6 0 0   V V         0 . 3 7 9 0     2 6 8 . 3 7 5 2 4         9 . 2 3 5 8 6       0 . 7 0 6 4 
 
     1 1       6 . 0 7 9   V V         0 . 6 9 9 6     5 8 3 . 5 6 8 1 2       1 0 . 2 6 0 0 5       1 . 5 3 6 0 
 
     1 2       7 . 8 9 2   V V         0 . 9 5 9 5     6 7 1 . 1 0 5 9 0         8 . 7 8 2 4 8       1 . 7 6 6 4 
 
     1 3       9 . 1 2 4   V V         0 . 8 3 5 5     5 4 8 . 6 7 0 7 2         8 . 0 8 7 1 7       1 . 4 4 4 1 
 
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 
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 
     1 6     1 1 . 2 7 8   B V         0 . 3 1 2 6     1 4 2 . 0 6 1 9 8         5 . 9 0 5 7 7       0 . 3 7 3 9 
 
     1 7     1 2 . 5 4 1   V V         0 . 3 4 5 5   4 1 2 6 . 1 3 5 2 5     1 8 1 . 3 3 9 4 6     1 0 . 8 6 0 2 
 
     1 8     1 4 . 2 0 2   V V         0 . 8 7 1 1     4 3 8 . 2 2 1 0 4         6 . 5 9 5 9 3       1 . 1 5 3 4 
 
     1 9     1 5 . 4 7 1   V B         0 . 5 7 9 8       8 2 . 9 0 5 6 9         1 . 7 2 7 9 4       0 . 2 1 8 2 
 
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 
     2 1     1 9 . 0 6 8   V B         0 . 3 7 5 9   5 6 4 0 . 9 8 2 4 2     2 3 5 . 1 3 1 9 0     1 4 . 8 4 7 3 
 
     2 2     2 0 . 9 7 8   B B         0 . 3 5 8 5   1 . 0 4 2 3 3 e 4       4 4 9 . 6 0 4 6 4     2 7 . 4 3 4 6 
 
     2 3     2 8 . 2 2 5   B B         0 . 3 6 2 8   1 . 1 7 2 5 6 e 4       5 0 5 . 1 6 5 8 3     3 0 . 8 6 2 3 
 
     2 4     3 6 . 6 6 0   B B         0 . 6 6 7 3       5 4 . 5 0 6 6 8         1 . 0 1 3 7 6       0 . 1 4 3 5 
 
 T o t a l s   :                                     3 . 7 9 9 3 2 e 4     1 5 5 1 . 6 1 8 0 6 
 
 
 
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 
                                                     * * *   E n d   o f   R e p o r t   * * * 
 
 