D a t a   F i l e   C : \ C H E M 3 2 \ 1 \ D A T A \ M A R I O \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 6 - 4 5 - 3 1 \ B E N Z O S _ 3 1 , 2 5 P P M . D 
 
 S a m p l e   N a m e :   b e n z o s _ 3 1 , 2 5 p p m 
 
 I n s t r u m e n t   1   6 / 2 1 / 2 0 2 3   9 : 3 5 : 2 9   P M   M a r i o 
 
 
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
 A c q .   O p e r a t o r       :   M a r i o                                                     S e q .   L i n e   :       4 
 
 A c q .   I n s t r u m e n t   :   I n s t r u m e n t   1                                         L o c a t i o n   :   V i a l   5 
 
 I n j e c t i o n   D a t e     :   6 / 2 1 / 2 0 2 3   8 : 3 5 : 1 2   P M                                   I n j   :       1 
 
                                                                                                 I n j   V o l u m e   :   1 5 . 0    l 
 
 S e q u e n c e   F i l e       :   C : \ C h e m 3 2 \ 1 \ D A T A \ M a r i o \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 6 - 4 5 - 3 1 \ B X _ S T D S _ E B _ 
 
                                     0 6 2 0 2 0 2 3 . S 
 
 M e t h o d                     :   C : \ C H E M 3 2 \ 1 \ D A T A \ M A R I O \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 6 - 4 5 - 3 1 \ E T H A N _ D T _ 
 
                                     M E O H _ L 1 6 - 6 . M   ( S e q u e n c e   M e t h o d ) 
 
 L a s t   c h a n g e d         :   6 / 5 / 2 0 2 3   1 0 : 4 9 : 1 0   A M   b y   M a r i o 
 
 M e t h o d   I n f o           :   S o l i d a g o   p h e n o l i c s   a n d   d i t e r p e n e   a c i d   a n a l y s i s 
 
 
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
                                                   A r e a   P e r c e n t   R e p o r t                                                   
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
 
 
 S o r t e d   B y                           :             S i g n a l 
 
 M u l t i p l i e r :                                       :             1 . 0 0 0 0 
 
 D i l u t i o n :                                           :             1 . 0 0 0 0 
 
 U s e   M u l t i p l i e r   &   D i l u t i o n   F a c t o r   w i t h   I S T D s 
 
 
 
 
 
 S i g n a l   1 :   D A D 1   A ,   S i g = 2 5 4 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 3 7 7   B V         0 . 2 7 3 2     2 9 3 . 8 4 5 6 7       1 3 . 3 2 9 8 1       6 . 1 8 8 1 
 
       2       2 . 5 1 6   V V         0 . 0 9 3 3     1 0 1 . 9 9 7 9 0       1 5 . 3 9 2 7 6       2 . 1 4 8 0 
 
       3       2 . 6 8 4   V V         0 . 0 8 5 5     1 0 8 . 0 8 5 7 6       2 0 . 5 2 0 1 7       2 . 2 7 6 2 
 
       4       2 . 8 0 2   V B         0 . 1 2 3 2     2 7 2 . 2 6 2 9 7       3 0 . 2 0 0 4 5       5 . 7 3 3 6 
 
       5       3 . 9 3 2   B V         0 . 9 0 7 2   1 1 0 9 . 7 8 5 1 6       1 4 . 9 6 3 9 1     2 3 . 3 7 0 9 
 
       6       5 . 1 0 3   V V         0 . 4 1 4 6     1 6 8 . 8 4 0 9 1         5 . 2 3 0 5 9       3 . 5 5 5 6 
 
       7     1 2 . 9 5 4   B V         0 . 3 3 3 3     9 4 0 . 1 2 3 8 4       4 4 . 0 0 0 2 0     1 9 . 7 9 8 0 
 
       8     1 9 . 7 0 3   B B         0 . 3 8 2 3   1 4 2 3 . 1 6 1 7 4       5 7 . 9 8 5 7 6     2 9 . 9 7 0 2 
 
       9     2 1 . 4 6 1   B B         0 . 3 5 9 6     2 4 1 . 1 6 4 9 2       1 0 . 3 5 8 7 1       5 . 0 7 8 7 
 
     1 0     2 8 . 8 3 8   B B         0 . 3 4 8 0       8 9 . 3 1 3 7 4         3 . 7 2 1 6 2       1 . 8 8 0 9 
 
 T o t a l s   :                                     4 7 4 8 . 5 8 2 6 2     2 1 5 . 7 0 3 9 9 
 
 
 
 
 
 S i g n a l   2 :   D A D 1   C ,   S i g = 3 2 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 3 7 1   B V         0 . 1 1 2 6       9 1 . 0 4 7 3 6       1 1 . 0 0 1 5 9     1 0 . 3 9 0 2 
 
       2       2 . 5 0 2   V V         0 . 0 9 8 8       9 8 . 7 2 8 3 7       1 5 . 3 9 9 4 2     1 1 . 2 6 6 7 
 
       3       2 . 6 7 8   V V         0 . 0 8 5 0     1 1 2 . 8 0 3 4 1       2 1 . 5 6 7 6 2     1 2 . 8 7 2 9 
 
       4       2 . 7 9 5   V B         0 . 1 0 0 6     2 0 5 . 8 6 2 6 6       2 8 . 3 7 6 8 2     2 3 . 4 9 2 7 
 
       5       3 . 8 6 5   B V         0 . 5 0 5 5     2 7 5 . 6 2 4 3 9         6 . 5 1 5 9 7     3 1 . 4 5 3 7 
 
       6       5 . 1 0 2   V V         0 . 2 6 3 5       7 0 . 1 7 5 3 0         3 . 6 6 2 5 3       8 . 0 0 8 3 
 
       7     1 9 . 6 9 0   B B         0 . 3 1 8 5       2 2 . 0 4 3 7 6   9 . 7 2 2 8 7 e - 1       2 . 5 1 5 6 
 
 T o t a l s   :                                       8 7 6 . 2 8 5 2 4       8 7 . 4 9 6 2 5 
 
 
 
 
 
 S i g n a l   3 :   D A D 1   D ,   S i g = 3 6 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 3 6 9   B V         0 . 1 0 7 6       9 1 . 0 2 6 4 1       1 1 . 5 8 7 3 2       9 . 7 7 0 8 
 
       2       2 . 5 0 0   V V         0 . 0 9 9 6     1 0 4 . 2 3 7 3 0       1 6 . 0 7 6 4 3     1 1 . 1 8 8 9 
 
       3       2 . 6 7 7   V V         0 . 0 8 5 1     1 2 4 . 4 0 9 1 6       2 3 . 7 5 8 8 4     1 3 . 3 5 4 2 
 
       4       2 . 7 9 3   V B         0 . 1 0 4 0     2 2 8 . 0 0 2 4 1       3 0 . 9 3 9 0 8     2 4 . 4 7 3 9 
 
       5       3 . 8 6 6   B V         0 . 5 1 0 7     2 9 5 . 0 3 7 7 8         7 . 0 1 5 3 2     3 1 . 6 6 9 5 
 
       6       5 . 1 0 8   V V         0 . 2 8 4 5       7 8 . 2 7 3 2 4         3 . 5 8 7 5 1       8 . 4 0 1 9 
 
       7       8 . 1 4 9   B B         0 . 3 1 4 8       1 0 . 6 2 7 3 3   4 . 3 8 4 2 1 e - 1       1 . 1 4 0 7 
 
 T o t a l s   :                                       9 3 1 . 6 1 3 6 2       9 3 . 4 0 2 9 2 
 
 
 
 
 
 S i g n a l   4 :   D A D 1   E ,   S i g = 2 1 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 1 4 3   B B         0 . 2 1 5 4       7 9 . 1 1 8 7 0         4 . 6 2 8 2 7       0 . 6 8 9 3 
 
       2       2 . 3 7 7   B V         0 . 1 1 4 7       5 3 . 1 6 7 2 4         6 . 2 8 2 8 9       0 . 4 6 3 2 
 
       3       2 . 5 2 8   V V         0 . 0 9 0 3       4 9 . 6 3 6 0 5         7 . 7 9 2 0 4       0 . 4 3 2 5 
 
       4       2 . 6 8 5   V V         0 . 0 8 0 9       5 2 . 0 5 8 2 6       1 0 . 6 6 4 9 9       0 . 4 5 3 6 
 
       5       2 . 8 0 2   V B         0 . 1 1 1 1     1 3 6 . 1 3 6 7 6       1 7 . 4 3 0 8 9       1 . 1 8 6 1 
 
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 
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 
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 
       9       6 . 0 0 8   V B         0 . 5 6 2 6     2 0 8 . 4 4 6 5 0         4 . 8 7 7 6 9       1 . 8 1 6 1 
 
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 
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 
     1 2     1 4 . 7 0 5   B B         0 . 4 3 5 2       5 0 . 8 0 8 9 7         1 . 7 2 7 3 4       0 . 4 4 2 7 
 
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 
     1 4     1 9 . 7 0 4   V B         0 . 3 8 3 6   3 8 9 2 . 4 5 7 5 2     1 5 7 . 8 9 8 2 7     3 3 . 9 1 2 9 
 
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 
     1 6     2 8 . 8 4 1   B B         0 . 3 6 6 2   1 8 2 9 . 8 7 3 2 9       7 7 . 8 4 5 0 7     1 5 . 9 4 2 7 
 
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 
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 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 3 7 8   B V         0 . 1 1 8 4       8 0 . 8 0 5 5 0         9 . 2 0 9 9 0       1 . 4 4 2 4 
 
       2       2 . 5 2 4   V V         0 . 1 0 6 5       7 5 . 8 6 3 2 4       1 1 . 8 6 7 1 1       1 . 3 5 4 1 
 
       3       2 . 6 8 6   V V         0 . 0 8 2 6       7 8 . 6 3 8 8 2       1 5 . 6 6 1 8 6       1 . 4 0 3 7 
 
       4       2 . 8 0 4   V B         0 . 1 2 3 4     2 1 9 . 0 9 0 5 8       2 4 . 7 1 9 2 5       3 . 9 1 0 7 
 
       5       3 . 8 4 1   B V         0 . 7 4 3 5     7 3 6 . 5 1 9 5 3       1 2 . 4 2 6 1 4     1 3 . 1 4 6 7 
 
       6       5 . 1 0 0   V V         0 . 3 6 8 4     1 4 7 . 8 3 6 6 9         5 . 1 8 9 2 6       2 . 6 3 8 8 
 
       7     1 2 . 9 5 4   B V         0 . 3 3 5 1     4 8 2 . 4 2 1 5 7       2 2 . 4 1 3 4 5       8 . 6 1 1 1 
 
       8     1 9 . 7 0 3   B B         0 . 3 7 7 7     7 3 2 . 6 6 8 2 1       2 9 . 9 1 4 4 5     1 3 . 0 7 7 9 
 
       9     2 1 . 4 6 1   B B         0 . 3 5 9 4   1 4 3 2 . 8 5 2 5 4       6 1 . 6 0 0 4 1     2 5 . 5 7 6 0 
 
     1 0     2 8 . 8 4 1   B B         0 . 3 6 6 2   1 6 1 5 . 6 2 5 2 4       6 8 . 7 4 4 6 9     2 8 . 8 3 8 5 
 
 T o t a l s   :                                     5 6 0 2 . 3 2 1 9 2     2 6 1 . 7 4 6 5 2 
 
 
 
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 
                                                     * * *   E n d   o f   R e p o r t   * * * 
 
 