D a t a   F i l e   C : \ C H E M 3 2 \ 1 \ D A T A \ M A R I O \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 5 - 2 2 - 3 5 \ B E N Z O S _ 5 0 0 P P M . D 
 
 S a m p l e   N a m e :   b e n z o s _ 5 0 0 p p m 
 
 I n s t r u m e n t   1   6 / 2 1 / 2 0 2 3   4 : 2 4 : 0 0   P M   M a r i o 
 
 
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
 A c q .   O p e r a t o r       :   M a r i o                                                     S e q .   L i n e   :       1 
 
 A c q .   I n s t r u m e n t   :   I n s t r u m e n t   1                                         L o c a t i o n   :   V i a l   1 
 
 I n j e c t i o n   D a t e     :   6 / 2 1 / 2 0 2 3   3 : 2 3 : 4 3   P M                                   I n j   :       1 
 
                                                                                                 I n j   V o l u m e   :   1 5 . 0    l 
 
 S e q u e n c e   F i l e       :   C : \ C h e m 3 2 \ 1 \ D A T A \ M a r i o \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 5 - 2 2 - 3 5 \ B X _ S T D S _ E B _ 
 
                                     0 6 2 0 2 0 2 3 . S 
 
 M e t h o d                     :   C : \ C H E M 3 2 \ 1 \ D A T A \ M A R I O \ B X _ S T D S _ E B _ 0 6 2 0 2 0 2 3   2 0 2 3 - 0 6 - 2 1   1 5 - 2 2 - 3 5 \ E T H A N _ D T _ 
 
                                     M E O H _ L 1 6 - 6 . M   ( S e q u e n c e   M e t h o d ) 
 
 L a s t   c h a n g e d         :   6 / 5 / 2 0 2 3   1 0 : 4 9 : 1 0   A M   b y   M a r i o 
 
 M e t h o d   I n f o           :   S o l i d a g o   p h e n o l i c s   a n d   d i t e r p e n e   a c i d   a n a l y s i s 
 
 
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
                                                   A r e a   P e r c e n t   R e p o r t                                                   
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
 
 
 S o r t e d   B y                           :             S i g n a l 
 
 M u l t i p l i e r :                                       :             1 . 0 0 0 0 
 
 D i l u t i o n :                                           :             1 . 0 0 0 0 
 
 U s e   M u l t i p l i e r   &   D i l u t i o n   F a c t o r   w i t h   I S T D s 
 
 
 
 
 
 S i g n a l   1 :   D A D 1   A ,   S i g = 2 5 4 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       1 . 9 4 2   B B         0 . 2 5 7 1     1 8 8 . 4 8 1 9 0         9 . 1 2 1 5 4       0 . 4 3 1 6 
 
       2       2 . 3 7 1   B V         0 . 1 1 6 0     1 3 4 . 3 5 0 1 0       1 5 . 6 7 5 5 1       0 . 3 0 7 6 
 
       3       2 . 5 2 1   V V         0 . 0 9 5 9     1 2 5 . 2 0 7 3 6       1 8 . 2 8 8 0 1       0 . 2 8 6 7 
 
       4       2 . 7 0 2   V V         0 . 1 0 1 8     1 4 2 . 9 2 0 7 9       2 3 . 2 1 4 0 0       0 . 3 2 7 3 
 
       5       2 . 7 9 5   V B         0 . 1 3 2 4     3 0 3 . 2 0 0 4 7       3 0 . 4 0 1 4 8       0 . 6 9 4 3 
 
       6       3 . 8 6 1   B V         0 . 8 3 1 4   1 4 1 8 . 5 0 2 2 0       2 0 . 4 9 8 0 3       3 . 2 4 8 1 
 
       7       5 . 0 8 3   V V         0 . 4 1 7 9     4 7 7 . 2 4 0 2 3       1 4 . 7 3 3 8 5       1 . 0 9 2 8 
 
       8       5 . 3 4 5   V V         0 . 2 1 4 8     1 8 8 . 4 6 4 6 6       1 2 . 7 2 4 5 2       0 . 4 3 1 6 
 
       9       5 . 6 2 5   V V         0 . 2 9 5 9     2 6 0 . 0 5 3 3 1       1 2 . 2 3 6 8 9       0 . 5 9 5 5 
 
     1 0       5 . 9 9 2   V V         0 . 7 1 9 7     6 6 6 . 5 3 0 3 3       1 1 . 1 4 5 7 2       1 . 5 2 6 2 
 
     1 1       7 . 3 0 3   V V         0 . 4 3 0 3     2 9 1 . 3 3 1 8 5         8 . 4 4 8 9 4       0 . 6 6 7 1 
 
     1 2       8 . 0 4 3   V V         0 . 7 3 8 6     4 2 0 . 3 4 0 0 0         6 . 9 7 9 7 5       0 . 9 6 2 5 
 
     1 3       9 . 7 1 7   V V         1 . 0 3 9 2     3 4 3 . 1 3 4 0 0         4 . 0 5 5 0 8       0 . 7 8 5 7 
 
     1 4     1 0 . 3 5 5   V V         0 . 4 8 4 5       9 7 . 8 7 9 7 6         2 . 4 2 6 9 9       0 . 2 2 4 1 
 
     1 5     1 2 . 1 0 2   B V         0 . 2 3 9 7       3 8 . 4 1 0 0 9         2 . 3 6 2 4 8       0 . 0 8 8 0 
 
     1 6     1 2 . 7 6 5   V B         0 . 3 2 1 2   1 . 3 1 5 1 6 e 4       6 3 6 . 0 8 9 2 9     3 0 . 1 1 4 9 
 
     1 7     1 4 . 4 7 4   B B         0 . 5 6 9 1     1 8 8 . 5 6 3 1 3         4 . 3 9 0 2 2       0 . 4 3 1 8 
 
     1 8     1 8 . 0 4 9   B V         0 . 3 6 7 9     1 3 3 . 7 4 9 9 2         5 . 3 4 5 0 0       0 . 3 0 6 3 
 
     1 9     1 9 . 3 4 1   V B         0 . 3 7 2 6   2 . 0 4 8 2 1 e 4       8 5 1 . 5 0 1 6 5     4 6 . 9 0 0 7 
 
     2 0     2 1 . 1 7 8   B B         0 . 3 6 9 3   3 3 7 5 . 2 5 7 8 1     1 3 9 . 9 9 1 2 3       7 . 7 2 8 8 
 
     2 1     2 8 . 4 5 9   B B         0 . 3 6 7 9   1 1 8 2 . 0 6 9 8 2       4 9 . 9 8 1 3 7       2 . 7 0 6 7 
 
     2 2     3 6 . 8 0 8   B V         0 . 3 6 7 4       6 1 . 8 8 8 1 5         2 . 6 2 2 1 4       0 . 1 4 1 7 
 
 T o t a l s   :                                     4 . 3 6 7 1 2 e 4     1 8 8 2 . 2 3 3 6 8 
 
 
 
 
 
 S i g n a l   2 :   D A D 1   C ,   S i g = 3 2 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 3 6 7   B V         0 . 1 0 3 8       9 3 . 1 5 5 0 1       1 2 . 1 0 2 0 0       5 . 1 6 5 9 
 
       2       2 . 5 0 4   V V         0 . 1 0 4 1     1 1 7 . 6 8 6 2 8       1 7 . 5 7 0 1 8       6 . 5 2 6 2 
 
       3       2 . 6 9 7   V V         0 . 1 0 4 0     1 3 8 . 9 5 7 5 0       2 2 . 5 1 9 4 0       7 . 7 0 5 8 
 
       4       2 . 7 8 9   V B         0 . 1 1 0 9     2 1 7 . 0 9 9 3 0       2 6 . 6 9 2 5 1     1 2 . 0 3 9 2 
 
       5       3 . 8 6 0   B V         0 . 5 3 7 5     2 7 0 . 0 9 5 2 8         6 . 3 5 9 2 6     1 4 . 9 7 8 0 
 
       6       5 . 0 8 6   V B         0 . 2 6 5 7     1 3 4 . 4 1 5 5 4         6 . 9 4 6 5 8       7 . 4 5 4 0 
 
       7       5 . 6 1 8   B V         0 . 2 9 6 4       7 9 . 5 5 7 9 4         3 . 7 3 6 1 1       4 . 4 1 1 9 
 
       8       6 . 1 1 1   V V         0 . 6 1 4 7     1 5 2 . 6 9 5 9 2         3 . 0 9 9 9 4       8 . 4 6 7 7 
 
       9     1 2 . 7 3 0   B B         0 . 2 9 1 5       3 5 . 4 5 4 8 8         1 . 7 1 2 6 3       1 . 9 6 6 1 
 
     1 0     1 4 . 4 7 9   B B         0 . 4 9 9 0     1 8 6 . 3 0 3 9 9         5 . 4 2 0 1 3     1 0 . 3 3 1 4 
 
     1 1     1 9 . 3 4 2   B B         0 . 3 6 6 1     3 4 9 . 5 5 6 6 7       1 4 . 6 6 3 2 3     1 9 . 3 8 4 5 
 
     1 2     2 1 . 6 1 0   B B         0 . 3 8 6 7       2 8 . 2 9 7 8 5   9 . 6 3 3 7 8 e - 1       1 . 5 6 9 2 
 
 T o t a l s   :                                     1 8 0 3 . 2 7 6 1 6     1 2 1 . 7 8 5 3 5 
 
 
 
 
 
 S i g n a l   3 :   D A D 1   D ,   S i g = 3 6 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
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 
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 
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 
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 
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 
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 
       7       5 . 6 1 1   V V         0 . 3 9 8 7       8 2 . 5 8 9 6 5         2 . 6 7 1 2 2       6 . 6 2 2 5 
 
       8     1 0 . 3 8 3   B B         0 . 3 8 3 8       1 3 . 9 2 0 9 9   4 . 5 1 4 2 7 e - 1       1 . 1 1 6 3 
 
       9     1 4 . 4 8 4   B B         0 . 5 4 9 3     1 5 9 . 4 1 3 2 4         3 . 6 0 9 1 3     1 2 . 7 8 2 6 
 
 T o t a l s   :                                     1 2 4 7 . 1 0 9 8 0     1 0 3 . 9 3 7 8 0 
 
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 
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 
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 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       1 . 9 4 2   B V         0 . 1 3 9 6       6 9 . 0 1 1 3 4         6 . 5 1 1 9 3       0 . 0 4 9 1 
 
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 
       3       2 . 3 6 6   V V         0 . 1 1 4 0       5 9 . 5 5 5 0 6         7 . 0 8 9 2 5       0 . 0 4 2 4 
 
       4       2 . 5 3 3   V V         0 . 0 9 2 7       5 4 . 7 4 8 8 0         8 . 3 2 4 0 0       0 . 0 3 9 0 
 
       5       2 . 7 0 2   V V         0 . 1 0 1 7       6 6 . 0 9 2 9 4       1 1 . 0 5 5 2 8       0 . 0 4 7 0 
 
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 
       7       3 . 8 3 6   B V         0 . 7 2 3 1     4 8 5 . 1 7 8 3 8         8 . 0 9 6 6 2       0 . 3 4 5 4 
 
       8       4 . 1 6 4   V B         0 . 1 7 1 4       9 9 . 1 1 1 1 0         7 . 8 4 6 8 3       0 . 0 7 0 6 
 
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 
     1 0       5 . 3 1 5   V V         0 . 1 6 3 8       3 4 . 8 7 2 8 3         3 . 1 8 4 0 4       0 . 0 2 4 8 
 
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 
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 
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 
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 
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 
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 
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 
     1 8     1 2 . 1 0 9   B V         0 . 3 2 4 7     2 0 3 . 4 5 5 7 8         8 . 7 0 5 8 5       0 . 1 4 4 8 
 
     1 9     1 2 . 7 6 5   V B         0 . 3 3 8 8   3 . 5 2 7 3 9 e 4     1 6 4 0 . 9 2 0 1 7     2 5 . 1 0 9 6 
 
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 
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 
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 
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 
     2 4     2 4 . 2 9 4   B V         0 . 3 4 4 4       2 0 . 3 4 1 4 5   9 . 5 5 3 4 5 e - 1       0 . 0 1 4 5 
 
     2 5     2 5 . 1 3 6   V B         0 . 3 6 7 3       4 6 . 1 0 3 3 6         1 . 7 9 6 8 4       0 . 0 3 2 8 
 
     2 6     2 8 . 4 5 8   B B         0 . 3 7 3 3   2 . 4 0 9 6 9 e 4     1 0 1 3 . 6 4 1 3 0     1 7 . 1 5 3 3 
 
     2 7     3 5 . 5 2 9   B B         0 . 3 9 1 4       3 3 . 6 2 5 9 7         1 . 1 5 5 7 4       0 . 0 2 3 9 
 
     2 8     3 6 . 8 1 2   B V         0 . 4 0 1 7     2 0 4 . 1 7 0 3 0         7 . 6 9 0 8 7       0 . 1 4 5 3 
 
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 
 T o t a l s   :                                     1 . 4 0 4 8 0 e 5     5 8 9 2 . 4 8 6 6 0 
 
 
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 
 
 S i g n a l   5 :   D A D 1   B ,   S i g = 2 3 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 1 2 4   B B         0 . 1 5 6 7       7 5 . 0 9 7 0 6         6 . 2 2 8 2 2       0 . 1 2 0 9 
 
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 
       3       2 . 5 2 9   V V         0 . 0 9 2 0       9 2 . 1 2 5 7 7       1 4 . 1 3 9 7 8       0 . 1 4 8 3 
 
       4       2 . 7 0 4   V V         0 . 1 0 1 2     1 0 0 . 9 1 3 3 1       1 7 . 0 1 3 2 0       0 . 1 6 2 4 
 
       5       2 . 7 9 8   V B         0 . 1 2 5 9     2 1 9 . 7 2 2 2 4       2 3 . 3 2 3 4 9       0 . 3 5 3 6 
 
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 
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 
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 
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 
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 
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 
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 
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 
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 
     1 8     1 4 . 4 7 6   B B         0 . 5 4 2 6     2 5 2 . 3 4 7 4 1         6 . 7 7 4 5 3       0 . 4 0 6 1 
 
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 
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 
     2 1     1 8 . 0 4 5   B V         0 . 3 9 7 0       7 3 . 4 0 9 8 3         2 . 7 0 2 1 5       0 . 1 1 8 1 
 
     2 2     1 9 . 3 4 1   V V         0 . 3 7 2 2   1 . 0 5 3 0 9 e 4       4 3 8 . 5 4 2 6 9     1 6 . 9 4 7 3 
 
     2 3     2 1 . 1 7 8   V B         0 . 3 6 2 4   1 . 9 2 5 2 0 e 4       8 1 8 . 3 9 7 5 8     3 0 . 9 8 2 1 
 
     2 4     2 4 . 3 3 9   B V         0 . 3 4 7 3       1 1 . 4 1 4 6 5   4 . 4 4 9 9 0 e - 1       0 . 0 1 8 4 
 
     2 5     2 8 . 4 5 8   B B         0 . 3 6 4 9   2 . 1 8 4 4 9 e 4       9 3 4 . 0 0 9 5 8     3 5 . 1 5 4 8 
 
     2 6     3 6 . 8 0 8   B V         0 . 3 6 9 4       3 2 . 5 9 8 0 0         1 . 3 5 1 4 2       0 . 0 5 2 5 
 
 T o t a l s   :                                     6 . 2 1 3 9 0 e 4     2 6 6 4 . 7 8 5 7 4 
 
 
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 
                                                     * * *   E n d   o f   R e p o r t   * * * 
 
 